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Soxhlet Extraction Unit

Soxhlet Extraction Unit

Soxhlet Extraction Unit

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A Soxhlet Extraction Unit is a laboratory apparatus used to extract soluble compounds (often lipids, oils, fats, or other desired compounds) from a solid material using a solvent. The process is continuous: solvent vaporizes, condenses, drips over the solid sample, dissolves the solute, and then returns (by siphoning) to the boiling flask — repeating the cycle many times.

Main Components

  • Boiling Flask: - Contains the solvent. When heated, the solvent vaporizes.
  • Soxhlet Extractor Body: - Has a chamber to hold a thimble (or other container) containing the solid sample. Solvent vapor enters, condenses and drips over the sample.
  • Condenser: - Cools the solvent vapour, so it condenses and returns into the extractor chamber.
  • Thimble: - A porous, usually filter-paper or cellulose one, which holds the solid sample and prevents solid particles from being washed into the boiling flask.
  • Heating System: - Could be a heating mantle, hot-plate, or bath (water or oil) depending on the design. It provides the heat to vaporize the solvent.
  • Support Structure / Frame: - Holds up the glassware securely — includes clamps, rods (vertical & horizontal), boss heads etc. Also, often a housing that may offer safety features.
  • Control / Regulation:- 
  1. Temperature control (thermostat, PID controller etc.) to maintain the right boiling/reflux conditions.
  2. Energy or power regulators etc.
  3. Sometimes timer or automation in more advanced units.
  • Cooling Water System:- To circulate water through the condenser to enable condensation of solvent vapours. The flow rate may be specified.

Parameters

Typical Range / Options

Number of parallel tests/positions

 

1, 3, 6 units (for doing more than one sample simultaneously)

Flask size (Solvent/boiling flask)

~ 50 ml up to several liters depending on size

Sample (extractor chamber) capacity

Similar to flask – depends on sample volume/rate needed

Max temperature / operating temperature

Some units go up to ~ 300-450°C for certain solvent systems or special glassware

Solvent recovery / closed system considerations

Some units are designed to recover > 80-90% of the solvent; some are automated to reduce loss and improve safety.

Power supply

Often 220-230 V AC, 50/60 Hz in many models; power rating depends on number of units and heating type.

Materials

Glassware (borosilicate etc.), metal frame (often mild steel), sometimes powder coated or epoxy coated for durability and resistance.

Heating type

Mantle, hot-plate, or water/oil bath.